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  Polymorphism and orientation control of copper-dicarboxylate metal–organic framework thin films through vapour- and liquid-phase growth

Rubio-Giménez, V., Carraro, F., Hofer, S., Fratschko, M., Stassin, T., Rodríguez-Hermida, S., Schrode, B., Barba, L., Resel, R., Falcaro, P., Ameloot, R. (2024): Polymorphism and orientation control of copper-dicarboxylate metal–organic framework thin films through vapour- and liquid-phase growth. - CrystEngComm, 26, 8, 1071-1076.
https://doi.org/10.1039/D3CE01296D

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???ViewItemFull_lblCiteItemAs???: https://gfzpublic.gfz.de/pubman/item/item_5025700 ???ViewItemFull_lblCiteItemVersionAs???: https://gfzpublic.gfz.de/pubman/item/item_5025700_2
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 ???ViewItemFull_lblCreators???:
Rubio-Giménez, Víctor1, ???ENUM_CREATORROLE_AUTHOR???
Carraro, Francesco1, ???ENUM_CREATORROLE_AUTHOR???
Hofer, Sebastian1, ???ENUM_CREATORROLE_AUTHOR???
Fratschko, Mario1, ???ENUM_CREATORROLE_AUTHOR???
Stassin, Timothée2, ???ENUM_CREATORROLE_AUTHOR???                 
Rodríguez-Hermida, Sabina1, ???ENUM_CREATORROLE_AUTHOR???
Schrode, Benedikt1, ???ENUM_CREATORROLE_AUTHOR???
Barba, Luisa1, ???ENUM_CREATORROLE_AUTHOR???
Resel, Roland1, ???ENUM_CREATORROLE_AUTHOR???
Falcaro, Paolo1, ???ENUM_CREATORROLE_AUTHOR???
Ameloot, Rob1, ???ENUM_CREATORROLE_AUTHOR???
???ViewItemFull_lblAffiliations???:
1External Organizations, ou_persistent22              
21.4 Remote Sensing, 1.0 Geodesy, Departments, GFZ Publication Database, Deutsches GeoForschungsZentrum, ou_146028              

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 ???ViewItemFull_lblAbstract???: Precise control over the crystalline phase and crystallographic orientation within thin films of metal–organic frameworks (MOFs) is highly desirable. Here, we report a comparison of the liquid- and vapour-phase film deposition of two copper-dicarboxylate MOFs starting from an oriented metal hydroxide precursor. X-ray diffraction revealed that the vapour- or liquid-phase reaction of the linker with this precursor results in different crystalline phases, morphologies, and orientations. Pole figure analysis showed that solution-based growth of the MOFs follows the axial texture of the metal hydroxide precursor, resulting in heteroepitaxy. In contrast, the vapour-phase method results in non-epitaxial growth with uniplanar texture only.

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 ???ViewItemFull_lblDates???: 20242024
 ???ViewItemFull_lblPublicationStatus???: ???ViewItem_lblPublicationState_published-in-print???
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 ???ViewItemFull_lblIdentifiers???: ???ENUM_IDENTIFIERTYPE_DOI???: 10.1039/D3CE01296D
???ENUM_IDENTIFIERTYPE_GFZPOF???: p4 T5 Future Landscapes
???ENUM_IDENTIFIERTYPE_GFZPOFCCA???: p4 CARF RemSens
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???ViewItemFull_lblSourceTitle???: CrystEngComm
???ViewItemFull_lblSourceGenre???: ???ENUM_GENRE_JOURNAL???, SCI, Scopus
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???ViewItemFull_lblSourcePubInfo???: ???lbl_noEntry???
???ViewItemFull_lblPages???: ???lbl_noEntry??? ???ViewItemFull_lblSourceVolumeIssue???: 26 (8) ???ViewItemFull_lblSourceSequenceNo???: ???lbl_noEntry??? ???ViewItemFull_lblSourceStartEndPage???: 1071 - 1076 ???ViewItemFull_lblSourceIdentifier???: ???ENUM_IDENTIFIERTYPE_CONE???: https://gfzpublic.gfz.de/cone/journals/resource/201610071
???ENUM_IDENTIFIERTYPE_PUBLISHER???: Royal Society of Chemistry (RSC)